How to strip dimethylformamide









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Removal Of Gas Phase Dimethylamine And

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And leaves a very obvious signal in the NMR even in trace amounts. See the link on this page entitled "Efficient extraction of highly polar solvents i. The product is an amide that also has an ester and a BOC group. I didn't notice it was resurrected from 3 years ago. In some cases the compounds was precipitating in water, so just collecting it on a frit, washing of the solid with water. A great trick to remove DMF via extraction is to wash your organic layer with an aqueous LiCl solution. We obtain low recovery when we attempt purification via extraction, and there are functional groups such as a carboxylic acid that give it more polarity than it would otherwise have. I've always had luck with just rotovap'ing it off with the highvac attached. Read This Before Posting. You can also remove most of the DMF under vacuum and then wash out the last traces. NotExactly on October 02, ,

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What is the best way to remove dimethylformamide (DMF) from a reaction mixture ? The product is an amide that also has an ester and a BOC.

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Description: In my experience, DMF is difficult to remove from reaction mixtures. I tried on a rotavap but it was not convenient. NotExactly on October 02, , I believe the reason is that the lithium coordinates between the carbonyl oxygen and nitrogen of DMF and pulls it into the aqueous layer. Don't forget that blowing it out works nicely too. See the link on this page entitled "Efficient extraction of highly polar solvents i. One suggestion we were given was to add water repeatedly and rotovap the mixed solvent with a Buchi V pump. And leaves a very obvious signal in the NMR even in trace amounts. You can find examples of this method in this paper. If it's quite polar you will probably lose some material, but in my experience the sacrifice is worth it. A great trick to remove DMF via extraction is to wash your organic layer with an aqueous LiCl solution. I've always had luck with just rotovap'ing it off with the highvac attached.
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