How to strip dimethylformamide
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Removal Of Gas Phase Dimethylamine And
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What are the methods for drying
And leaves a very obvious signal in the NMR even in trace amounts. See the link on this page entitled "Efficient extraction of highly polar solvents i. The product is an amide that also has an ester and a BOC group. I didn't notice it was resurrected from 3 years ago. In some cases the compounds was precipitating in water, so just collecting it on a frit, washing of the solid with water. A great trick to remove DMF via extraction is to wash your organic layer with an aqueous LiCl solution. We obtain low recovery when we attempt purification via extraction, and there are functional groups such as a carboxylic acid that give it more polarity than it would otherwise have. I've always had luck with just rotovap'ing it off with the highvac attached. Read This Before Posting. You can also remove most of the DMF under vacuum and then wash out the last traces. NotExactly on October 02, ,
What is the best way to remove dimethylformamide (DMF) from a reaction mixture ? The product is an amide that also has an ester and a BOC.
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